Abstracts of Paper's Submitted for Publication


In the following:

  1. M.I. Nelson Flammability limits in closed vessel experiments: A Semenov model. Submitted, 2000.
  2. M.I. Nelson and X.D. Chen. Heterogeneously catalysed combustion in a continuously stirred tank reactor. II Autothermal behaviour in low temperature reactions. Submitted, 2000.
  3. M.I. Nelson, R.O. Weber and A.G. Tate. Modelling of Open Vat Red Wine Fermenters. Submitted, 2002.
  4. X.D. Chen and M.I. Nelson. Modelling Air-Drying of Coal Particles - A New Biot and Lewis Number Analysis. Submitted, 2005.
  5. H.S. Sidhu, S.D. Watt, and M.I. Nelson. Performance comparison between a two-reactor cascade and a single tank in an Activated Sludge Wastewater Treatment Process. Accepted for publication in the International Journal of Environment and Waste Management, 11th April 2007.
  6. S.D. Watt, H.S. Sidhu, M.I. Nelson, A.K. Ray. Analysis of a model for ethanol production through continuous fermentation in multiple tanks. Submitted, 2008.
  7. M.I. Nelson, H.S. Sidhu and X.D. Chen. The passage of food through animal stomachs: A chemical reactor engineering approach. Submitted, 2008.
  8. M.I. Nelson, H.S. Sidhu and A.A. Adesina. An operational model for a well-stirred membrane bioreactor: reactor performance analysis. Submitted, 2008.
  9. M.I. Nelson, E. Balakrishnan and and H.S. Sidhu. A fundamental analysis of continuous flow bioreactor and membrane reactor models with Tessier kinetics Submitted, 2008.
  10. M.I. Nelson and H.S. Sidhu. Flammability limits of an oxidation reaction in a batch reactor. Submitted, 2008.
  11. M.I. Nelson and T.C.L. Yuem. A fundamental analysis of a membrane bioreactor containing a sludge disintegration system. Submitted, 2008.
  12. M.I. Nelson, H.S. Sidhu and A.A. Adesina. Analysis of an immobilised enzyme reactor model. Submitted, 2008.
  13. S.D. Watt, H.S. Sidhu, M.I. Nelson and A.K. Ray. Analysis of a model for ethanol production through continuous fermentation: ethanol productivity. Submitted, 2008.
  14. M.I. Nelson, H.S. Sidhu and A.A. Adesina. Analysis of an immobilised enzyme reactor model with catalyst activation. Submitted, 2008.

Flammability limits in closed vessel experiments: A Semenov model

Abstract:

The standard Semenov model is extended to incorporate flammability experiments in which oxygen-fuel-inert mixtures are assembled in a closed vessel at a specified initial pressure and temperature.

The model contains three generic steady-state diagrams: unique; isola; and, mushroom. Of these the mushroom response represents the most severe hazard. The three types of response arise as the system is unfolded from a winged cusp singularity by varying the nitrogen fraction and/or the ambient temperature. A complete unfolding of this singularity is not possible as it is degenerate.

The isola steady-state structure contains two extinction limit points which define the lower and upper flammability limits. Unfolding these points with secondary bifurcation parameters mimics certain experimental procedures revealing qualitatively agreement between theory and experiment.

Keywords: boundary bifurcation, flammability limits, isola, singularity theory, winged-cusp.

M.I. Nelson. Flammability limits in closed vessel experiments: A Semenov model. Submitted, 2000.


Heterogeneously catalysed combustion in a continuously stirred tank reactor. II Autothermal behaviour in low temperature reactions

Abstract

In this paper we investigate autothermal behaviour in a catalytic reactor as a function of the coolant temperature. Under specified conditions it is shown that fixing the coolant temperature and heating the catalyst is equivalent to fixing the power and varying the coolant temperature.

As the inflow concentration of the reactant is increased from zero there is a critical value at which a cusp singularity occurs. Below criticality there is a unique stable steady-state. Above criticality the steady-state diagram exhibits the classic S-shaped response curve. Above criticality three types of catalytic behaviour are distinguished, depending upon the values of the coolant temperature at the extinction and ignition points. These are: non-autothermal behaviour, autothermal behaviour, and self-ignition. The crossover points from non-autothermal to autothermal behaviour and from autothermal to self-ignition are defined by boundary bifurcations.

Keywords: autothermal, boundary bifurcation, catalytic reactors.

M.I. Nelson and X.D. Chen. Heterogeneously catalysed combustion in a continuously stirred tank reactor. II Autothermal behaviour in low temperature reactions Submitted, 2000.


Modelling of Open Vat Red Wine Fermenters

Abstract

We model the extraction of polyphenolic compounds from grape skins during the fermentation of grape juice. Our first model is based upon current experimental practice and consists of a porous layer of grape skins sitting on top of the fermenting juice. To maintain wetness of the grape skins, which is required for extraction of polyphenolic compounds which give red wine its character and quality, fermenting juice is poured over the grape skins. We assume that the current process of wetting the grapes for half an hour in a six hour period over seven days is equivalent to a continuous operation of fourteen hours. In the second model we consider a new reactor configuration in which the cap is placed in a separate reactor to the fermenting juice and recirculation is not used. For both models we investigate how the performance of the system, as measured by the fractional extraction, depends upon the flowrate and total run-time. We find that the the system without recirculation has the potential to significantly decrease the total processing time.

Keywords: continuously stirred tank reactor; fermentation; polyphenols.

M.I. Nelson, R.O. Weber and A.G. Tate. Modelling of Open Vat Red Wine Fermenters. Submitted 2002.


Modelling Air-Drying of Coal Particles - A New Biot and Lewis Number Analysis

Abstract

Previously coal drying has been modelled using a moving boundary analysis with two approaches: one assuming that heat transfer is limiting and one considering the diffusion of water vapor in a dry shell but still having a moving sharp evaporation interface. In this paper, a new Biot number and Lewis number analysis is presented showing that there is a likelihood for a mass transfer limiting process to occur depending on the parameter ranges such as particle size and drying air temperature etc. Under certain circumstances, it may be more fundamentally correct to assume a uniform temperature distribution and to solve a PDE for effective water transfer. Alternatively, the simultaneous heat and mass transfer PDEs can be solved in order to account for the physics properly.

X.D. Chen and M.I. Nelson. Modelling Air-Drying of Coal Particles - A New Biot and Lewis Number Analysis. Submitted, 2005.


Performance comparison between a two-reactor cascade and a single tank in an Activated Sludge Wastewater Treatment Process

Abstract

We investigate a model for the treatment of wastewater in the activated sludge process. The process is based on the aeration of waste water with flocculating biological growth, followed by the separation of treated waste water from biological growth. Part of this growth is then wasted, and the remainder is returned to the system. The biochemical model consists of two types of bacteria, sludge bacteria and sewage bacteria, and two types of ciliated protozoa, free-swimming ciliates and ciliates attached to sludge flocs. A combination of steady-state analysis, path following techniques and numerical integration of the governing equations are used to study the dynamics of this system in a network of two coupled reactors arranged in a series. We compare the treatment efficiency for a single tank system with that of a two-reactor cascade. In the latter scenario the total residence time is fixed and the residence time in the first reactor is taken to be a design parameter. Process parameters that ensure optimal performance are discussed.

Keywords: wastewater treatment, activated sludge process, bifurcation, treatment efficient, reaction engineering, stability, modelling.

S.D. Watt, H.S. Sidhu and M.I. Nelson. Wastewater Treatment by Activated Sludge Process: comparing the performance of a two-reactor cascade with a single tank. Accepted for publication in the International Journal of Environment and Waste Management, 11th April 2007.




Analysis of a model for ethanol production through continuous fermentation in multiple tanks

Abstract

We investigate an experimentally verified model for the production of ethanol through continuous fermentation. Previous studies have investigated this model using direct integration. This approach is time consuming as parameter regions of interest can only be determined through laborious and repetitive calculations. Using techniques from nonlinear dynamical systems theory, in particular a combination of steady-state analysis and path following methods, practical insights into operating strategies can be found. The optimisation of ethanol productivity is considered here.

S.D. Watt, H.S. Sidhu, M.I. Nelson, A.K. Ray. Analysis of a model for ethanol production through continuous fermentation in multiple tanks. Submitted, 2008.


The passage of food through animal stomachs: A chemical reactor engineering approach

Abstract

In many circumstances it is useful to know the mean residence time of food substrates within the body following digestion. For instance, such information is crucial to estimate the extent to which dietary components are fermented inside animal stomaches. The mean residence time can be estimated by measuring the rate at which non-absorbable markers, mixed as a supplement into an animals food, are deposited in the animals faces. The experimental data are analysed with the use of an appropriate mathematical model.

We analyse multicompartmental models for the flow of digesta along the gastrointestinal tract of animals. The problem can be treated as a sequence of `tanks' in series. Of interest is the fact that the volume of the tanks is not necessarily constant. For example, following digestion of food, secretion of pancreatic juices may occur; diluting the tracer. Thus the problem can be treated as a series of semi-batch reactors in series.

This problem is a good illustration of the application of the methods of chemical reactor engineering to a situation that, at first sight, does not appear to be a chemical engineering problem.

M.I. Nelson, H.S. Sidhu and X.D. Chen. The passage of food through animal stomachs: A chemical reactor engineering approach. Submitted, 2008.


An operational model for a well-stirred membrane bioreactor: reactor performance analysis

Abstract

We investigate the behaviour of a reaction described by Michaelis-Menten kinetics in an immobilised enzyme reactor (IER). The IER is treated by a well-stirred flow reactor, in which the bound and unbounded enzyme species are immobilised and therefore constrained to remain within the reaction vessel. The product species leaves the bioreactor either in the reactor outflow or by permeating through the semi-permeable reactor wall. We explore how the concentration of recovered product and the reactor productivity vary with process parameters, particularly those associated with the separation of the product from the substrate through the semi-permeable reactor wall.

We show that at low residence times membrane extraction through the reactor walls increases the total product concentration recovered whereas at high residence times membrane extraction decreases the total product concentration. We also show that the reactor productivity is maximised at high residence times. For reactor productivity the key control variable is the ratio of the reactor volume to the jacket volume (V*). If this ratio is greater than one, then membrane extraction increases the productivity. If this ratio is less than one, then membrane extraction decreases the productivity.

M.I. Nelson, H.S. Sidhu and A.A. Adesina. An operational model for a well-stirred membrane bioreactor: reactor performance analysis. Submitted, 2008.


A fundamental analysis of continuous flow bioreactor and membrane reactor models with Tessier kinetics

Abstract

In this research we analyze the steady-state operation of a continuous flow bioreactor, with or without recycle, and an idealised, or non-idealised, continuous flow membrane reactor. The model extends to include a fixed bed reactor where a fraction of the biomass is detached by the flow. The reaction is assumed to be governed by Tessier growth kinetics. We show that a flow reactor with idealised recycle has the same performance as an idealised membrane reactor and that the performance of a non-idealised membrane reactor is identical to an appropriately defined continuous flow bioreactor with non-idealised recycle. The performance of all three reactor types can therefore be obtained by analyzing a flow reactor with recycle. The steady-states of the recycle model are found and their stability determined as a function of the residence time. The performance of the reactor at large residence times is obtained.

Keywords: bioreactor; kinetics; membrane reactor; modelling; stirred tank .

M.I. Nelson, E. Balakrishnan and and H.S. Sidhu. A fundamental analysis of continuous flow bioreactor and membrane reactor models with Tessier kinetics Submitted, 2008.


Flammability limits of an oxidation reaction in a batch reactor

Abstract

When reactant consumption is ignored the flammability limits of a fuel-oxygen mixture may be identified as bifurcation points on a steady-state diagram. When reactant consumption is included there is no longer a clear-cut definition of criticality. We investigate the flammability of a simple global mechanism for oxidation in a batch reactor. Regions of super- and sub-criticality are distinguished using sensitivity analysis.

It is numerically convenient to reduce problems in two-dimensions to one-dimension. This can be done formally through the use of centre manifold techniques, or informally using physical reasoning. We investigate the extent to which diabatic two-dimensional problems may be accurately represented by a one-dimensional model.

Keywords: centre manifold theory, sensitivity analysis, thermal explosions.

M.I. Nelson and H.S. Sidhu. Flammability limits of an oxidation reaction in a batch reactor. Submitted 2008.


A fundamental analysis of a membrane bioreactor containing a sludge disintegration system

Abstract

We analyze the steady-state operation of a membrane bioreactor system (MR) incorporating a sludge disintegration unit (SD). The latter is used to prevent excess sludge production. The relationship between process control parameters and the performance of the MR-SD is determined by finding the steady-states of the model and determining their stability as a function of the residence time. Asymptotic solutions for the steady-state solutions in the limit of high residence times are obtained. These show that at sufficiently high residence times the mixed liquor suspended solids (MLSS) content of the bioreactor is independent of the operation of the sludge disintegration unit. Thus the main role played by the sludge disintegration unit is to improve the performance at `low' residence times. For a specified MLSS concentration the values of the dimensionless residence time and the sludge disintegration factor are determined that ensure zero excess sludge production. If the sludge disintegration factor is sufficiently high then the MLSS content is guaranteed to be below the target value (`negative' excess sludge production) provided that the residence time is higher than the washout value. It is shown that zero excess sludge production can be achieved with a slight decrease in effluent quality.

Keywords: activated sludge; membrane bioreactor; modelling; sludge disintegration; sludge reduction; stirred tank; wastewater treatment.

M.I. Nelson and T.C.L. Yuem. A fundamental analysis of a membrane bioreactor containing a sludge disintegration system Submitted, 2008.


Analysis of an immobilised enzyme reactor model

Abstract

We investigate the behaviour of a reaction described by Michaelis-Menten kinetics in an immobilised enzyme reactor (IER). The IER is treated as a well-stirred flow reactor, in which the immobilised bounded and unbounded enzyme species are constrained to remain within the reaction vessel. The product species leaves the IER in the reactor outflow. Before the substrate can react with the enzyme, the enzyme must first be activated by absorption of an activator. We use steady-state analysis to identify the best operating conditions for the reactor. To this end we show that the concentration of product is maximised at low residence times whereas the productivity of the reactor is maximised at high residence times.

Keywords: Bioreactors; Nonlinear Dynamics; Reaction Engineering .

M.I. Nelson, H.S. Sidhu and A.A. Adesina. Analysis of an immobilised enzyme reactor model. Submitted, 2008.


Analysis of a model for ethanol production through continuous fermentation: ethanol productivity

Abstract

We investigate a model for the production of ethanol through continuous fermentation using Saccharomyces cerevisiae in a single reactor and cascades of upto five reactors. Using path-following methods we investigate how the ethanol productivity varies with the residence time in each reactor of the cascade. With a substrate feed concentration of 160 g/l we find the optimal productivity is 3.80 g/l/h, 5.08 g/l/h, and 5.18 g/l/h in a single reactor, a double reactor cascade and a triple reactor cascade respectively. For the case of a cascade containing reactors of equal size we investigate reactor configurations of up to five reactors and find that the maximum productivity is obtained in a cascade containing three reactors.

Keywords: ethanol, modelling, productivity, reactor cascade. .

S.D. Watt, H.S. Sidhu, M.I. Nelson and A.K. Ray. Analysis of a model for ethanol production through continuous fermentation: ethanol productivity. Submitted, 2008.



Analysis of an immobilised enzyme reactor model with catalyst activation

Abstract

We investigate the behaviour of a reaction described by Michaelis-Menten kinetics in an immobilised enzyme reactor (IER). The IER is treated as a well-stirred flow reactor, in which the immobilised bounded and unbounded enzyme species are constrained to remain within the reaction vessel. The product species leaves the IER in the reactor outflow. Before the substrate can react with the enzyme, the enzyme must first be M

activated by absorption of an activator.

We use steady-state analysis to identify the best operating conditions for the reactor. To this end we show that the concentration of product is maximised at low residence times whereas the productivity of the reactor is maximised at high residence times.

Keywords: Bioreactors; Nonlinear Dynamics; Reaction Engineering .

M.I. Nelson, H.S. Sidhu and A.A. Adesina. Analysis of an immobilised enzyme reactor model with catalyst activation. Submitted, 2008.


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