NMR Instrumentation
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Inova 500-MHz NMR Spectrometer
- Main features:
- Oxford super conductor 500 MHz magnet;
- A triple-channel spectrometer with a triple-axis pulsed-field gradient module and a waveform generator;
- A 34-channel shim module;
- An FTS variable temperature preconditioner and stabiliser with 0.05o precision from -40o to +60o;
- VNMR 6.1c software on SUN Solaris 9 operating system.
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Three probes are available for this spectrometer:
- 5mm 1H / 13C / 15N triple-nucleus triple-gradient probe;
- 8mm DOTY broadband diffusion probe;
- 4mm 1H / 13C indirect-detection z-gradient nano probe, which uses ~40 micro-litre of sample.
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Mercury VX 300-MHz NMR Spectrometer
Main features:
- Oxford super conductor 300 MHz magnet;
- A two-channel broadband system with a Performa I pulsed field gradient (PFG) module.
- A 14-channel shim module;
- A variable temperature controller with 0.1oC precision between −80oC to +150oC;
- SMS 50 auto-sample changer;
- VNMR 6.1c software on SUN Solaris 9 operating system.
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Two probes are available for this spectrometer:
- auto-switchable 4-nuclear (1H/19F/31P/13C) 5mm z-gradient probe;
- 1H/19F/31P/13C 5mm PFG, 4-nuclear probe.
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VNMRS PS54 500-MHz NMR Spectrometer
Main features:
- Varian super conductor 500 MHz, 54-mm bore, shielded magnet;
- A 28-channel shim module for high performance non-spin line shape;
- DirectDrive architecture with optimal RF control and implementation;
- Dual-channel High/Low Band module;
- Performa IV DirectDrive PFG module;
- A variable temperature unit with 0.1oC precision between −4oC to +60oC for liquid samples;
- Protune Accessary – Dual Drive Module;
- Vnmrj 2.1B software on Linux operating system.
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Three probes are available for this spectrometer:
- 1H {15N - 31P} 5mm PFG, AutoX Indirect Detect probe, 500 MHz NB;
- 15N – 31P{1H} 4-mm Broadband NANO probe, VT, 500 NB;
- 1H – 19F / 15N – 31P 5mm PFG AutoX DB Probe.
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Last reviewed: 27 April, 2007